Fia-Cl Determination of Paracetamol Using Luminol–Kmno4–Pb Post-Cl System, Applying Merging Zone Principle
Keywords:
post-Chemiluminescence, flow injection analysis, paracetamolAbstract
This paper reports a new and simple flow injection analysis (FIA) with post- chemiluminescence system (PCL) for determination of paracetamol through merging zone principle. The method was based on the inhibition of luminol–KMnO4–Pb post- chemiluminescence (PCL).Various parameters associated with this flow system were studied and essential optimizations were carried out. Calibration graph were constructed for determination of paracetamol in the range (5.0–30) μg.ml-1 with correlation coefficient (0.996) .The method was applied successfully for the determination of paracetamol in commercial pharmaceutical products.
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References
Afkhami, A. (2006). "Spectrophotometric Determination of Salicylamide and Paracetamol in Biological Samples and Pharmaceutical Formulations by a Differential Kinetic Method " Acta Chim. Slov. 53: 357–362.
Alapont, A. G. (1999). "Indirect determination of paracetamol in pharmaceutical formulations by inhibition of the system luminol-H2O2-Fe(CN)3-(6) chemiluminescence." J. Pharm. Biomed. Anal., 21(2): 311-317.
Du J and Lu J. (2004 ,). "Hydrazine-induced post-chemiluminescence phenomenon of permanganate-luminol reaction and its applications ,." Luminescence , 19 ,(6 ,): 328-332 .
Easwaramoorthy, D. (2001). "Chemiluminescence detection of paracetamol by a luminol-permanganate based reaction." Anal. Chim. Acta 439: 95-100.
Afkhami, A. (2006). "Spectrophotometric Determination of Salicylamide and Paracetamol in Biological Samples and Pharmaceutical Formulations by a Differential Kinetic Method " Acta Chim. Slov. 53: 357–362.
Alapont, A. G. (1999). "Indirect determination of paracetamol in pharmaceutical formulations by inhibition of the system luminol-H2O2-Fe(CN)3-(6) chemiluminescence." J. Pharm. Biomed. Anal., 21(2): 311-317.
Du J and Lu J. (2004 ,). "Hydrazine-induced post-chemiluminescence phenomenon of permanganate-luminol reaction and its applications ,." Luminescence , 19 ,(6 ,): 328-332 .
Easwaramoorthy, D. (2001). "Chemiluminescence detection of paracetamol by a luminol-permanganate based reaction." Anal. Chim. Acta 439: 95-100.
Esmail, W. A. (2004). Flow injection chemiluminsecence for the determination of some nitrogen containing compounds, . Department of chemistry, University of Salahaddin. Ph.D.: 124.
Florey, K. (2003). "Analytical profilesof drug substances." Elsevier 8: 424-451.
Godse, V. P. (2009). "Reverse Phase HPLC Method for Determination of Aceclofenac and Paracetamol in Tablet Dosage Form." Asian J. Research Chem. 2(1): 37- 40.
Hua, C. (2002). "Determination of paeacetamol by flow injection chemiluminescence analysis." Chinese J. Analyt. Chem 11.
Idris, A. M. (2005). "Sequential injection spectrophotometric kinetic method for the determination of Paracetamol in dosage forms " J. Flow Injection Anal. 22(2): 123–128.
Jabbar, H. S. (2006). Flow injection analysis with chemiluminescence and spectrophotometric detection for determination of some pharmacetucal formulations. Department of chemistry University of Salahaddin. M.Sc.thesis: 52
Koukli, I. I. and Hadjiioannou, T. P. (1989). "Continuous-flow chemiluminescence determination of acetaminophen by reduction of cerium(IV)." Analyst 114: 711-714.
Kumar, P. and Khan, Z. (2006). "Unusual stabilization of water-soluble colloidal MnO2 during the oxidation of paracetamol by MnO4- " Polym Sci 284(10): 1155-1162.
Nagendra, P. (2011). "Spectrophotometric Estimation of Paracetamol in Bulk and Pharmaceutical Formulations." E-Journal of Chemistry 8(1): 149-152.
Oliveira, M. C. Q. (2010). "Flow injection analysis of paracetamol using a biomimetic sensor as a sensitive and selective amperometric detector." Anal. Methods 2( 5): 507-512.
Pan, J. (2007). "Effect of pH on the characteristics of potassium permanganate–luminol CL reaction in the presence of trace aluminum(III) and its analytical application." Talanta 71(5): 1861–1866.
Ruengsitagoon, W. (2006). "Flow injection chemiluminescence determination of paracetamol." Talanta 69(4): 976.
Shi-qian, W. ( 2011). "Reversed Flow Injection Inhibition Chemiluminescence System for the Determination of Paracetamol." Journal of Jiangxi Normal University, 3: 15.
Shrestha, B. R. and Pradhananga, R. R. (2009). "Spectrophotometric Method for the Determination of Paracetamol." J. Nepal Chem. Soc 24: 39.
Shu-min, W. (2011). "Flow injection chemiluminescence determination of paracetamol with chromium(VI)-H202-luminol system." Chinese J. Anal. Lab. 4: 32.
Sultan, S. M. (2004). "Sequential Injection Spectrophotometric Method for the Assay of Paracetamol in Drug Formulations " J. Flow Injection Anal. 21(1).
Tavallali, H. and Hamid, Y. ( 2011). "Spectrofluorometric determination of Paracetamol in pharmaceutical formulations." Asian Journal of Biochemical and Pharmaceutical Research (AJPCR) 1(2): 2231.
Vogel, A. ( 1979). London.
Zhao, S. (2006). "Detection of paracetamol by capillary electrophoresis with chemiluminsecence detection." Anal. Chim. Acta 559 195.
Alapont, A. G. (1999). "Indirect determination of paracetamol in pharmaceutical formulations by inhibition of the system luminol-H2O2-Fe(CN)3-(6) chemiluminescence." J. Pharm. Biomed. Anal., 21(2): 311-317.
Du J and Lu J. (2004 ,). "Hydrazine-induced post-chemiluminescence phenomenon of permanganate-luminol reaction and its applications ,." Luminescence , 19 ,(6 ,): 328-332 .
Easwaramoorthy, D. (2001). "Chemiluminescence detection of paracetamol by a luminol-permanganate based reaction." Anal. Chim. Acta 439: 95-100.
Afkhami, A. (2006). "Spectrophotometric Determination of Salicylamide and Paracetamol in Biological Samples and Pharmaceutical Formulations by a Differential Kinetic Method " Acta Chim. Slov. 53: 357–362.
Alapont, A. G. (1999). "Indirect determination of paracetamol in pharmaceutical formulations by inhibition of the system luminol-H2O2-Fe(CN)3-(6) chemiluminescence." J. Pharm. Biomed. Anal., 21(2): 311-317.
Du J and Lu J. (2004 ,). "Hydrazine-induced post-chemiluminescence phenomenon of permanganate-luminol reaction and its applications ,." Luminescence , 19 ,(6 ,): 328-332 .
Easwaramoorthy, D. (2001). "Chemiluminescence detection of paracetamol by a luminol-permanganate based reaction." Anal. Chim. Acta 439: 95-100.
Esmail, W. A. (2004). Flow injection chemiluminsecence for the determination of some nitrogen containing compounds, . Department of chemistry, University of Salahaddin. Ph.D.: 124.
Florey, K. (2003). "Analytical profilesof drug substances." Elsevier 8: 424-451.
Godse, V. P. (2009). "Reverse Phase HPLC Method for Determination of Aceclofenac and Paracetamol in Tablet Dosage Form." Asian J. Research Chem. 2(1): 37- 40.
Hua, C. (2002). "Determination of paeacetamol by flow injection chemiluminescence analysis." Chinese J. Analyt. Chem 11.
Idris, A. M. (2005). "Sequential injection spectrophotometric kinetic method for the determination of Paracetamol in dosage forms " J. Flow Injection Anal. 22(2): 123–128.
Jabbar, H. S. (2006). Flow injection analysis with chemiluminescence and spectrophotometric detection for determination of some pharmacetucal formulations. Department of chemistry University of Salahaddin. M.Sc.thesis: 52
Koukli, I. I. and Hadjiioannou, T. P. (1989). "Continuous-flow chemiluminescence determination of acetaminophen by reduction of cerium(IV)." Analyst 114: 711-714.
Kumar, P. and Khan, Z. (2006). "Unusual stabilization of water-soluble colloidal MnO2 during the oxidation of paracetamol by MnO4- " Polym Sci 284(10): 1155-1162.
Nagendra, P. (2011). "Spectrophotometric Estimation of Paracetamol in Bulk and Pharmaceutical Formulations." E-Journal of Chemistry 8(1): 149-152.
Oliveira, M. C. Q. (2010). "Flow injection analysis of paracetamol using a biomimetic sensor as a sensitive and selective amperometric detector." Anal. Methods 2( 5): 507-512.
Pan, J. (2007). "Effect of pH on the characteristics of potassium permanganate–luminol CL reaction in the presence of trace aluminum(III) and its analytical application." Talanta 71(5): 1861–1866.
Ruengsitagoon, W. (2006). "Flow injection chemiluminescence determination of paracetamol." Talanta 69(4): 976.
Shi-qian, W. ( 2011). "Reversed Flow Injection Inhibition Chemiluminescence System for the Determination of Paracetamol." Journal of Jiangxi Normal University, 3: 15.
Shrestha, B. R. and Pradhananga, R. R. (2009). "Spectrophotometric Method for the Determination of Paracetamol." J. Nepal Chem. Soc 24: 39.
Shu-min, W. (2011). "Flow injection chemiluminescence determination of paracetamol with chromium(VI)-H202-luminol system." Chinese J. Anal. Lab. 4: 32.
Sultan, S. M. (2004). "Sequential Injection Spectrophotometric Method for the Assay of Paracetamol in Drug Formulations " J. Flow Injection Anal. 21(1).
Tavallali, H. and Hamid, Y. ( 2011). "Spectrofluorometric determination of Paracetamol in pharmaceutical formulations." Asian Journal of Biochemical and Pharmaceutical Research (AJPCR) 1(2): 2231.
Vogel, A. ( 1979). London.
Zhao, S. (2006). "Detection of paracetamol by capillary electrophoresis with chemiluminsecence detection." Anal. Chim. Acta 559 195.
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Published
2013-09-30
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Science Journal of University of Zakho
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Fia-Cl Determination of Paracetamol Using Luminol–Kmno4–Pb Post-Cl System, Applying Merging Zone Principle. (2013). Science Journal of University of Zakho, 1(2), 723-734. https://sjuoz.uoz.edu.krd/index.php/sjuoz/article/view/377
